Erice, Italy, 2-12 June 2011
Structural crystallography is often thought to be synonymous with single-crystal crystallography, yet for several decades, powder diffraction has made important contributions to the understanding of materials structure and behaviour. However, it is perhaps the last decade that has seen some of the most remarkable breakthroughs in experimental powder diffraction and in the analysis of powder diffraction data, to the extent that it is no longer considered to be an analytical technique of last resort. Instrumentation at both the laboratory and facility level has become increasingly versatile to the extent that throughput and resolution are no longer mutually exclusive. In the field of data analysis, ingenious algorithms that take full advantage of modern computing power have meant that inorganic, molecular and even protein structures are being solved and refined relatively routinely. The 44th crystallographic course at the Ettore Majorana Centre was intended to serve as a complete introduction to the diverse field of powder diffraction, and to provide a firm grounding for attendees, from which to build future research achievements.
These presentations are also available on YouTube
Photograph © Peter Mueller 2011
Day 1 - Fundamentals
Introduction
Martin Schmidt: Introduction to Erice (with Photos)
Videos
- Bill David: Introduction to the Course (18 min 16 sec)
- Bill David: Powder Diffraction - by Decades (41 min 36 sec)
- Kenneth Shankland: Data Collection - Good Practices (48 min 53 sec)
- Peter W. Stephens: Indexing Powder Diffraction Data (44 min 20 sec)
- Peter W. Stephens: Rietveld Refinement (48 min 16 sec)
- Lynne McCusker: Structure Solution Overview (54 min 02 sec)
- Radovan Cerny: Inorganic Materials (46 min 11 sec)
- Kenneth Shankland: Organic Materials (61 min 53 sec)
Day 2 - Instrumentation at the Frontiers
- Pamela Whitfield: Laboratory X-ray Diffraction (53 min 40 sec)
- Fabia Gozzo: Synchrotron X-ray Diffraction (49 min 04 sec)
- Laurent Chapon: Neutron Powder Diffraction (46 min 32 sec)
- Andy Fitch: Ultrafast Powder Diffraction (49 min 27 sec)
- Colin Pulham: Taking it to Extremes (49 min 42 sec)
- Laurent Chapon: Introduction to Fullprof (45 min 16 sec)
- Bob Von Dreele: Introduction to GSAS and GSAS-II (29 min 54 sec)
- (PDF version)
Day 3 - Structure Solution
- Carmelo Giacovazzo: Structure Solution Using Direct Methods (49 min 21 sec)
- Chris Gilmore: Structure Solution Using Maximum Entropy Methods
- Lukas Palatinus: Structure Solution Using Charge Flipping (48 min 25 sec)
- Kenneth Shankland: Structure Solution Via Global Optimization Methods (48 min 02 sec)
- Angela Altomare: Introduction to EXPO (47 min 42 sec)
- Radovan Cerny: Introduction to Fox (40 min 41 sec)
Day 4 - Big Challenges
- Jon Wright: Proteins and Powders - Technical Developments (49 min 02 sec)
- Irene Margiolaki: Proteins and Powders - An Overview (49 min 23 sec)
- Joel Bernstein: Pharmaceuticals and Powders - An Overview (50 min 32 sec)
- Bill David: Parametric Powder Diffraction (48 min 05 sec)
Day 5 - Powder Plus
- Christian Baerlocher: Powder Diffraction and Electron Microscopy - A Powerful Combination (no sound) (36 min 17 sec)
- (PDF version)
- Yaroslav Filinchuk: In-situ Powder Diffraction (no sound) (11 min 29 sec)
- Laurent Chapon: Powder Diffraction and Magnetism (25 min 03 sec)
- Lubo Smrcok: Computational Methods (32 min 34 sec)
- Kenneth Shankland: DASH (32 min 34 sec)
- Lukas Palatinus: Superflip (13 min 37 sec)
- Arnt Kern: TOPAS (40 min 46 sec)
Day 6 - Less Than Perfect
- Matteo Leoni: Imperfections (14 min 37 sec)
- Tamás Ungár: Faulting (40 min 26 sec)
- (PDF version)
- Simon Billinge: Atomic Pair Distribution Function Analysis (13 min 12 sec)
- Yuri Andreev: Debye Analysis (37 min 20 sec)
Day 7 - Quantitative
- Ian Madsen: Quantitative Phase Analysis
- Arnt Kern: Quantifying Amorphous Phases (44 min 17 sec)
- Luca Lutterotti: Quantitative Phase Analysis (43 min 33 sec)
Day 8 - Texture: Friend and Foe
- Bob Von Dreele: Introduction to Texture (47 min 21 sec)
- Christian Baerlocher: Texture and Structure Solutio (40 min 52 sec)
- (PDF version)
- Gilberto Artioli: Powder Diffraction and Cultural Heritage (50 min 27 sec)
- (PDF version)
- Xun-Li Wang: Railway Lines to Airbus Wings (48 min 45 sec)
- Luca Lutterotti: Introduction to MAUD (52 min 53 sec)
- Rietveld Refinement and MAUD (PDF)