Supplementary videos for Journal of Applied Crystallography

ks0017sup1.mpg
Tetragonal-rhombohedral (orientation)
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ks0017sup2.mpg
Tetragonal-rhombohedral (sin [delta])
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ks0017sup3.mpg
Cubic-tetragonal (orientation)
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ks0017sup4.mpg
Cubic-tetragonal (sin [delta])
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he5319sup10.avi
Supplementary material
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he5319sup11.avi
Supplementary material
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he5319sup12.avi
Supplementary material
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he5319sup13.avi
Supplementary material
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he5319sup14.avi
Supplementary material
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he5319sup15.avi
Supplementary material
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he5319sup16.avi
Supplementary material
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he5319sup17.avi
Supplementary material
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he5319sup4.avi
Supplementary material
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he5346sup2.avi
Supplementary material
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he5346sup3.avi
Supplementary material
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he5346sup4.avi
Supplementary material
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he5319sup5.avi
Supplementary material
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he5319sup6.avi
Supplementary material
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he3456sup5.avi
Supplementary material
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he5319sup7.avi
Supplementary material
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he5346sup6.avi
Supplementary material
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he5319sup8.avi
Supplementary material
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he5319sup9.avi
Supplementary material
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he5346sup7.avi
Supplementary material
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he5374sup1.avi
M1: Background-corrected raw projection data acquired during scan A.
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he5374sup2.avi
M2: Background-corrected raw projection data acquired during scan B.
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he5374sup3.avi
M3: A three-dimensional rendition of the grain surface, obtained from the reconstruction of scan A.
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cj6012sup1.avi
Time-resolved movie of the evolution of the speckle patterns as the particles move within the sample. The movie frequency is 50 times real time. The top-left corner is the Q = 0 position, covered by the beamstop.
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hx5063sup1.avi
Supplementary material
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he5462sup1.mpg
Overall view of the procedure of using the device. The black CCD camera at the center of this view supported by a three-finger clamp is temporarily set for the microscopic up view of the crystal.
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hx5063sup2.avi
Supplementary material
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he5444sup2.avi
Process of crystal manipulation
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he5462sup2.mpg
Closeup view of the procedure. A protein crystal was picked up from a drop and frozen. In this demonstration, the drop was put on a cover slide, but it is possible to pick a crystal up from crystallization plates.
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he5462sup3.mpg
Demonstration of the movement of the mechanically linked X-Y-Z micromanipulator. The tilt angle of the cryo-pin is adjustable by an optical encoder attached at the manipulator arm.
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he5462sup4.mpg
Demonstration of synchronously-controlled cryo-stream shutter and manipulator. The action repeats twice.
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he5462sup5.mpg
Real time movie of the microscopic view of the tip of the capillary at the freezing position. It is possible to see the process of removing the external solution. A hen egg white lysozyme crystal was used.
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he5462sup6.avi
20% slow-motion movie of he5462sup5.mpg. It is easily observed that the external solution is aspirated and the crystal sits on the tip of the capillary just before freezing.
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he5462sup7.mpg
Real time movie of the microscopic view of a hen egg white lysozyme crystal.
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he5462sup8.mpg
Real time movie of the microscopic view of a thaumatin crystal.
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he5462sup9.mpg
A thaumatin crystal. One end of the crystal sticks into the capillary hole.
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he5470sup1.avi
The robot in action
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he5480sup1.wmv
Real-time fitting of data for RT3
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ea5129sup2.wmv
Video 1: Preparation of the Nextal tray
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ea5129sup3.wmv
Video 2: Incorporating magnets for loop manipulation
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wf5079sup1.wmv
Intensity BIM video for sample VTE28
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wf5079sup2.wmv
Orientation BIM video for sample VTE28
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wf5079sup3.wmv
sin delta BIM video for sample VTE28
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wf5079sup4.wmv
Intensity BIM video for sample LNT67
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wf5079sup5.wmv
Orientation BIM video for sample LNT67
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wf5079sup6.wmv
sin delta BIM video for sample LNT67
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ce5128sup1.avi
A series of topography images at different diffraction angles from an undoped single-crystal CVD diamond displaying almost no parasitic scattering (the same one as in Figs. 2 and 5e).
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ce5128sup2.avi
A series of topography images at different diffraction angles from a single-crystal CVD diamond displaying strong parasitic scattering (the same one as in Figs. 4c and 5f).
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ks5305sup1.wmv
Temperature dependence of optical birefringence and distribution of orientation angles in the pure NBT crystal. See Figs. 2-3 for more details. High-resolution version.
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ks5305sup2.wmv
Temperature dependence of optical birefringence and distribution of orientation angles in the Mn-doped NBT crystal. See Figs. 5-6 for more details. High-resolution version.
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ks5305sup3.wmv
Temperature dependence of optical birefringence in the pure NBT crystal. See Fig. 2 for more details. High-resolution version.
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ks5305sup4.wmv
Temperature dependence of optical birefringence in the Mn-doped NBT crystal. See Fig. 5 for more details. High-resolution version.
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ks5305sup5.avi
Temperature dependence of optical birefringence and distribution of orientation angles in the pure NBT crystal. See Figs. 2-3 for more details. Low-resolution version.
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ks5305sup6.avi
Temperature dependence of optical birefringence and distribution of orientation angles in the Mn-doped NBT crystal. See Figs. 5-6 for more details. Low-resolution version.
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ks5305sup7.avi
Temperature dependence of optical birefringence in the pure NBT crystal. See Fig. 2 for more details. Low-resolution version.
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ks5305sup8.avi
Temperature dependence of optical birefringence in the Mn-doped NBT crystal. See Fig. 5 for more details. Low-resolution version.
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aj5201sup1.wmv
Combined SAXS and 3DXRD patterns
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he5568sup1.mov
Movie S1: progression of the precipitation front. Four TollN6-VLR capillaries were set up with reservoirs either of 3.4 M sodium malonate pH 7.0 (two capillaries on the left) or 0.15M I3C, 2.89M sodium malonate pH 7.0 (two capillaries on the right). A picture was taken every hour over ten days. A movie was generated with 24 frames per second. The progression of the precipitation front is clearly visible in the second capillary from the left.
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xk5009sup1.avi
Movie 1
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xk5009sup2.avi
Movie 2
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xz5004sup1.wmv
Movie showing X-ray diffraction images around a crack tip during heating
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